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2026 (Current Year) Faculty Courses School of Materials and Chemical Technology Undergraduate major in Materials Science and Engineering

Metallurgical Engineering Laboratory III

Academic unit or major
Undergraduate major in Materials Science and Engineering
Instructor(s)
Shinji Muraishi / Kenichi Kawamura / Azusa Ooi / Takashi Harumoto / Yoshihiro Terada / Shintaro Yasui / Naoki Nohira / Takumi Kosaba / Hiroyuki Dannoshita / Jundong Song / Ryutaro Matsumura / Takashi Watanabe / Tomoyuki Kurioka / Ryota Nagashima
Class Format
Experiment
Media-enhanced courses
-
Day of week/Period
(Classrooms)
Class
-
Course Code
MAT.M352
Number of credits
002
Course offered
2026
Offered quarter
4Q
Syllabus updated
Mar 9, 2026
Language
Japanese

Syllabus

Course overview and goals

Course Overview
Metallurgical engineering is a broad discipline that encompasses various fields, including metal physics, metal chemistry, metal materials science, and metal processing. In this laboratory course, students will learn fundamental experimental techniques and analytical methods essential for metallurgical engineering. Specifically, they will gain hands-on experience in evaluating the physical, chemical, and mechanical properties of metals and develop the ability to analyze the characteristics of different materials from a scientific perspective. Through discussions based on experimental results, students will also enhance their understanding of the properties of metallic materials from a materials science viewpoint.

Course Objectives
This course aims to provide students with systematic training in experimental techniques in metallurgical engineering and deepen their understanding of both theoretical and practical aspects. Students will explore how the physical and chemical properties of metals influence material characteristics and investigate the relationship between microstructure and properties. Additionally, they will develop essential skills in data processing, analysis, and technical report writing, which are crucial for effectively communicating their findings.

Course description and aims

1. Fabrication and Characterization of Thin Metal Films
Understand the evaporation process of silver and gold thin films and measure their electrical resistivity and optical properties.
2. Evaluation of Magnetic Properties of Metallic Materials
Assess the magnetic properties of metallic materials using vibrating sample magnetometry (VSM).
3. Understanding Corrosion and Electrochemical Properties of Metals
Understand the principles of immersion copper plating and electrolytic copper plating and conduct related experiments.
4. Evaluation of Molten Pig Iron Desulfurization by Slag
To understand the principles of hot metal desulfurization by slag and the method for measuring sulfur concentration using the combustion analysis method.
5. Evaluation of Mechanical Properties and Their Dependence on Temperature and Strain Rate
Perform tensile tests under different temperature and strain rate conditions to understand the thermally activated process of dislocations.
Analyze the stress-strain response of structural materials and investigate its relationship with microstructure.
6. Evaluation of Low-Cycle Fatigue Fracture of Materials
To conduct low-cycle fatigue tests on steel materials, acquire the measurement techniques, and understand the deformation behavior under cyclic loading.
7. Enhancement of Discussion and Presentation Skills
Summarize experimental results and present and discuss findings.

Keywords

Thin Metal Films, Vapor Deposition, Electrical Resistivity, Optical Properties, Magnetic Properties, Vibrating Sample Magnetometry (VSM), Corrosion, Polarization Curve, Desulfurization reaction, Mechanical Properties, Stress-Strain Characteristics, Strain Rate Dependency, Thermally Activated Process of Dislocations, Microstructural Control, Material Design

Competencies

  • Specialist skills
  • Intercultural skills
  • Communication skills
  • Critical thinking skills
  • Practical and/or problem-solving skills

Class flow

Grouping and the schedule for the experiments will be announced by principle instructor.

Course schedule/Objectives

Course schedule Objectives
Class 1

General introduction

To understand contents of general introduction

Class 2

Thin metal films (Day 1)

1. To understand the fundamental principles of the vacuum vapor deposition.
2. To learn how to measure the electrical resistivity using the four-terminal method.
3. To analyze the relationship between deposition time and electrical resistivity.

Class 3

Thin metal films (Day 2)

1. To learn how to measure the electrical resistivity using the four-probe method.
2. To analyze the relationship between film thickness and electrical resistivity.

Class 4

Magnetization behavior of ferromagnetic alloy by means of VSM I : Ni and Ni-Cu alloys

To measure the magnetization behavior of ferromagnetic alloy (Ni and Ni-Cu) by means of vibration sample magnetometer.

Class 5

Magnetization behavior of ferromagnetic alloy by means of VSM II : Magnetic crystal anisotropy of pure Fe single crystal

To measure the magnetization behavior of pure iron single crystal by means of vibration sample magnetometer.

Class 6

Electrochemical reaction I : immersion copper plating

To understand the mechanism of immersion copper plating.

Class 7

Electrochemical reaction II : electrolytic copper plating

To learn electrolytic copperplating techniques.

Class 8

Desulfurization of pig iron using slag (Sample Preparation)

To enable High temperature oxidation of metal, and its sample preparation.

Class 9

Desulfurization of pig iron using slag (Sample Analysis)

To understand the combustion method for sulfur content and the mechanism of desulfurization from pig iron.

Class 10

Mechanical properties I: Tensile testing of pure metals at different temperatures and strain rates

To understand the effects of differences in crystal structure and temperature on mechanical properties.

Class 11

Mechanical Properties II: Tensile testing of practical alloy materials at room temperature

To deepen understanding of the mechanisms of metal strengthening.

Class 12

Low Cycle Fatigue Fracture of Steel I: Understanding of Fatigue fracture, Use of Strain Gauge, Axial Loading Test by Strain Gauge

To enable students to understand characteristics of fatigue fracture and its difference from tensile fracture.

Class 13

Low Cycle Fatigue Fracture of Steel II: Low Cycle Fatigue Test and Fatigue Life Prediction

To enable students to understand the cyclic stress-strain behavior of materials.

Class 14

[Materials] General discussion and presentation

To make presentation and discussion about experiments.

Study advice (preparation and review)

To enhance effective learning, students are encouraged to spend approximately 50 minutes preparing for class and another 50 minutes reviewing class content afterwards (including assignments) for each class.
They should do so by referring to textbooks and other course material.

Textbook(s)

The lecture materials will be distributed by your teacher on the day of the lecture or you can download the lecture materials for each topic from the ‘Science Tokyo LMS’ system and bring them with you.

Reference books, course materials, etc.

nothing in particular

Evaluation methods and criteria

Participation and reports are taken into account for the score.

Related courses

  • MAT.M351 : Metallurgical Engineering Laboratory II

Prerequisites

Nothing particular