2024 Faculty Courses School of Materials and Chemical Technology Department of Chemical Science and Engineering Graduate major in Chemical Science and Engineering
Advanced Instrumental Analysis
- Academic unit or major
- Graduate major in Chemical Science and Engineering
- Instructor(s)
- Toshiro Takao / Kenichi Ozawa / Satoka Aoyagi / Manabu Hoshino /
- Class Format
- Lecture (Face-to-face)
- Media-enhanced courses
- -
- Day of week/Period
(Classrooms) - 5-8 Wed
- Class
- -
- Course Code
- CAP.A481
- Number of credits
- 100
- Course offered
- 2024
- Offered quarter
- 4Q
- Syllabus updated
- Mar 14, 2025
- Language
- Japanese
Syllabus
Course overview and goals
[Summary of the course] In this course, mass spectrum, single crystal X-ray structural analysis, infrared spectroscopic analysis, and chemical analysis using X-ray are explained.
[Aim of the course] Identification of compounds is essential for any field of chemistry. In this course, principles of the analytical methods and characterization of the analytical data are explained. Recent progress of the analytical techniques is also described.
Course description and aims
By the end of this course, students acquire the following ability:
(1) Ability to explain the principles of the spectroscopic analyses.
(2) Ability to interpret the results of the spectroscopic analysis.
(3) Ability to explain recent progress on analytical techniques.
Keywords
mass spectroscopy, single crystal X-ray structural analysis, infrared spectroscopy, X-ray photoelectron spectroscopy (XPS), X-ray absorption spectroscopy (XAS), extended X-ray absorption fine structure (EXAFS)
Competencies
- Specialist skills
- Intercultural skills
- Communication skills
- Critical thinking skills
- Practical and/or problem-solving skills
Class flow
This course will overview the contents of (1) mass spectrum, (2) single crystal X-ray structural analysis, (3) infrared spectroscopy, and chemical analysis using X-ray (including synchrotron).
In 2023, 12/6 Mass spectroscopy, 12/20 XPS, 1/10 Single crystal XRD, 1/17 Infrared spectroscopy.
Course schedule/Objectives
| Course schedule | Objectives | |
|---|---|---|
| Class 1 | Fundamentals of single crystal X-ray structural analysis | Ability to explain the principles of single crystal X-ray crystallography. |
| Class 2 | Application of single crystal X-ray structural analysis | Ability to interpret the results of single crystal X-ray structural analysis. |
| Class 3 | Fundamentals of mass spectroscopy | Ability to explain the principles of mass spectroscopy. |
| Class 4 | Application of mass spectroscopy | Ability to interpret the results of mass spectroscopy |
| Class 5 | X-ray photoelectron spectroscopy (XPS) Fundamentals of mass spectroscopy | Ability to explain the principles of XPS and interpret the spectra. |
| Class 6 | X-ray absorption spectroscopy (XAS), extended X-ray absorption fine structure (EXAFS) Application of mass spectroscopy | Ability to explain the principles of XAS and EXAFS and interpret the spectra. |
| Class 7 | Fundamentals of infrared spectroscopy | Ability to explain the principles of infrared spectroscopy. |
| Class 8 | Practical of infrared spectroscopy | Ability to interpret the infrared spectra. |
Study advice (preparation and review)
To enhance effective learning, students are encouraged to spend approximately 100 minutes preparing for class and another 100 minutes reviewing class content afterwards (including assignments) for each class.
They should do so by referring to textbooks and other course material.
Textbook(s)
None required.
Reference books, course materials, etc.
Course materials are provided during class.
Evaluation methods and criteria
Practice problems and interpretation for confirming the level of understanding or quality of writing reports (50%), level of class participation (50%) (The level of class participation will be assessed by discussion, small examination and so on in the lecture.)
Related courses
- CAP.A421 ： Advanced Design of Organic Reaction Processes I
- CAP.A422 ： Advanced Design of Organic Reaction Processes I
- CAP.A461 ： Advanced Solid State Chemistry I
- CAP.A462 ： Advanced Solid State Chemistry II
- CAP.A465 ： Advanced Bioinorganic Chemistry I
- CAP.A466 ： Advanced Bioinorganic Chemistry II
- CAP.T531 ： Advanced Catalytic Reactions I
- CAP.T532 ： Advanced Catalytic Reactions II
- CAP.A423 ： Advanced Organic Synthesis I
- CAP.A424 ： Advanced Organic Synthesis II
Prerequisites
It is desirable to study the related courses.
Contact information (e-mail and phone) Notice : Please replace from ”[at]” to ”@”(half-width character).
Toshiro TAKAO : takao.t.aa[at]m.titech.ac.jp
Office hours
Contact by e-mail in advance to schedule an appointment.
Other
The schedule will be announced once fixed.